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1 Supplementary Information J. Braz. Chem. Soc., Vol. 00, No. 00, S1-S14, Printed in Brazil Sociedade Brasileira de Química $ SI Fábio S. Grasel,*,a,b Fabiano Barreto, c Louise Jank a,c and Valter Stefani*,a a Instituto de Química, Universidade Federal do Rio Grande do Sul, CP 15003, Porto Alegre-RS, Brazil b Programa de Pós-graduação em Engenharia e Tecnologia de Materiais, Pontifícia Universidade Católica do Rio Grande do Sul, CP 1429, Porto Alegre-RS, Brazil c Laboratório Nacional Agropecuário - LANAGRO/RS, Ministério da Agricultura, Pecuária e Abastecimento, Porto Alegre-RS, Brazil Figure S1. IR spectrum (nujol) of compound 3a. Figure S3. IR spectrum (nujol) of compound 3c Figure S2. IR spectrum (nujol) of compound 3b. Figure S4. IR spectrum (nujol) of compound 3d. * fsgrasel@gmail.com, vstefani@iq.ufrgs.br

2 S2 J. Braz. Chem. Soc / a.u. 0.8 Figure S5. IR spectrum (nujol) of compound 4a. Figure S8. IR spectrum (nujol) of compound 4d. Figure S6. IR spectrum (nujol) of compound 4b. Figure S9. IR spectrum (nujol) of compound 5a. 0.8 Figure S7. IR spectrum (nujol) of compound 4c. Figure S10. IR spectrum (nujol) of compound 5b.

3 Vol. 00, No. 00, 2015 Grasel et al. S3 Figure S11. IR spectrum (nujol) of compound 5c. Figure S12. IR spectrum (nujol) of compound 5d. Figure S13. 1 H NMR spectrum (300 MHz, DMSO-d 6 ) of compound 3a.

4 S4 J. Braz. Chem. Soc. Figure S14. 1 H NMR spectrum (300 MHz, DMSO-d 6 ) of compound 3a. Figure S15. 1 H NMR spectrum (300 MHz, DMSO-d 6 ) of compound 3b.

5 Vol. 00, No. 00, 2015 Grasel et al. S5 Figure S16. 1 H NMR spectrum (300 MHz, DMSO-d 6 ) of compound 3b. Figure S17. 1 H NMR spectrum (300 MHz, DMSO-d 6 ) of compound 3c.

6 S6 J. Braz. Chem. Soc. Figure S18. 1 H NMR spectrum (300 MHz, DMSO-d 6 ) of compound 3c. Figure S19. 1 H NMR spectrum (300 MHz, DMSO-d 6 ) of compound 3d.

7 Vol. 00, No. 00, 2015 Grasel et al. S7 Figure S20. 1 H NMR spectrum (300 MHz, DMSO-d 6 ) of compound 3d. Figure S21. 1 H NMR spectrum (300 MHz, DMSO-d 6 ) of compound 4a.

8 S8 J. Braz. Chem. Soc. Figure S22. 1 H NMR spectrum (300 MHz, DMSO-d 6 ) of compound 4a. Figure S23. 1 H NMR spectrum (300 MHz, DMSO-d 6 ) of compound 4b.

9 Vol. 00, No. 00, 2015 Grasel et al. S9 Figure S24. 1 H NMR spectrum (300 MHz, DMSO-d 6 ) of compound 4b. Figure S25. 1 H NMR spectrum (300 MHz, DMSO-d 6 ) of compound 4c.

10 S10 J. Braz. Chem. Soc. Figure S26. 1 H NMR spectrum (300 MHz, DMSO-d 6 ) of compound 4c. Figure S27. 1 H NMR spectrum (300 MHz, DMSO-d 6 ) of compound 4d. Figure S28. 1 H NMR spectrum (300 MHz, DMSO-d 6 ) of compound 4d.

11 Vol. 00, No. 00, 2015 Grasel et al. S11 Figure S29. 1 H NMR spectrum (300 MHz, DMSO-d 6 ) of compound 5a. Figure S30. 1 H NMR spectrum (300 MHz, DMSO-d 6 ) of compound 5a.

12 S12 J. Braz. Chem. Soc. Figure S31. 1 H NMR spectrum (300 MHz, DMSO-d 6 ) of compound 5b. Figure S32. 1 H NMR spectrum (300 MHz, DMSO-d 6 ) of compound 5b.

13 Vol. 00, No. 00, 2015 Grasel et al. S13 Figure S33. 1 H NMR spectrum (300 MHz, DMSO-d 6 ) of compound 5c. Figure S34. 1 H NMR spectrum (300 MHz, DMSO-d 6 ) of compound 5c.

14 S14 J. Braz. Chem. Soc. Figure S35. 1 H NMR spectrum (300 MHz, DMSO-d 6 ) of compound 5d. Figure S36. 1 H NMR spectrum (300 MHz, DMSO-d 6 ) of compound 5d.

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Supplementary Information

Supplementary Information J. Braz. Chem. Soc., Vol. 21, No. 8, S1-S23, 2010. Printed in Brazil - 2010 Sociedade Brasileira de Química 0103-5053 $6.00+0.00 Francisco E. A. Rodrigues, a Jefferson Q. Lima, a,b Maria da Conceição F.