Artigo. doi number. Quim. Nova, Vol. XY, No. 00, 1-21, 200_. Salacia crassifolia (Celastraceae): CHEMICAL CONSTITUENTS AND ANTIMICROBIAL ACTIVITY

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1 Quim. Nova, Vol. XY, No. 00, 1-21, 200_ doi number Salacia crassifolia (Celastraceae: CHEMICAL CONSTITUENTS AND ANTIMICROBIAL ACTIVITY Vanessa G. Rodrigues a, *, Lucienir P. Duarte a, Roqueline R. Silva b, Grácia D. F. Silva a, Maria O. Mercadante-Simões c, Jacqueline A. Takahashi a, Bibiane L. G. Matildes a, Thaisa H. S. Fonseca d, Maria A. Gomes d and Sidney A. Vieira Filho e a Departamento de Química, Instituto de Ciências Exatas, Universidade Federal de Minas Gerais, Belo Horizonte MG, Brasil b Departamento de Química, FACET, Universidade Federal dos Vales do Jequitinhonha e Mucuri, Campus II - Alto da Jacuba, Diamantina MG, Brasil c Departamento de Biologia Geral, Universidade Estadual de Montes Claros, Campus Universitário Professor Darcy Ribeiro, Montes Claros MG, Brasil d Departamento de Parasitologia, Instituto de Ciências Biológicas, Universidade Federal de Minas Gerais, Belo Horizonte MG, Brasil e Departamento de Farmácia, Escola de Farmácia, Universidade Federal de Ouro Preto, Ouro Preto MG, Brasil Artigo Figure 1S. 1 H NMR spectrum of compound 1 (200 MHz, CDCl 3 * vanessa.greg@yahoo.com

2 S2 Rodrigues et al. Quim. Nova Figure 2S. 13 C NMR spectrum of compound 1 (50 MHz, CDCl 3 Figure 3S. DEPT-135 NMR spectrum of compound 1 (50 MHz, CDCl 3

3 Vol. XY, No. 00 Salacia crassifolia (Celastraceae: chemical constituents and antimicrobial activities S3 Figure 4S. 1 H NMR spectrum of compound 2 (400 MHz, CDCl 3 Figure 5S. 13 C NMR spectrum of compound 2 (100 MHz, CDCl 3

4 S4 Rodrigues et al. Quim. Nova Figure 6S. DEPT-135 NMR spectrum of compound 2 (100 MHz, CDCl 3 Figure 7S. 1 H NMR spectrum of compound 3 (400 MHz, CDCl 3

5 Vol. XY, No. 00 Salacia crassifolia (Celastraceae: chemical constituents and antimicrobial activities S5 Figure 8S. 13 C NMR spectrum of compound 3 (100 MHz, CDCl 3 Figure 9S. DEPT-135 NMR spectrum of compound 3 (100 MHz, CDCl 3

6 S6 Rodrigues et al. Quim. Nova Figure 10S. Mass spectrum with the molecular ion at m/z 409 (C + of compound 3 Figure 11S. Mass spectrum with the molecular ion at m/z 255 (C - of compound 3

7 Vol. XY, No. 00 Salacia crassifolia (Celastraceae: chemical constituents and antimicrobial activities S7 Figure 12S. 1 H NMR spectrum of compound 4 (400 MHz, CDCl 3 Figure 13S. 13 C NMR spectrum of compound 4 (100 MHz, CDCl 3

8 S8 Rodrigues et al. Quim. Nova Figure 14S. DEPT-135 NMR spectrum of compound 4 (100 MHz, CDCl 3 Figure 15S. 1 H NMR spectrum of compound 5 (400 MHz, CDCl 3 + Pyridine-d5

9 Vol. XY, No. 00 Salacia crassifolia (Celastraceae: chemical constituents and antimicrobial activities S9 Figure 16S. 13 C NMR spectrum of compound 5 (100 MHz, CDCl 3 + Pyridine-d5 Figure 17S. DEPT-135 NMR spectrum of compound 5 (100 MHz, CDCl 3 + Pyridine-d5

10 S10 Rodrigues et al. Quim. Nova Figure 18S. 1 H NMR spectrum of compound 6 (400 MHz, CDCl 3 Figure 19S. 13 C NMR spectrum of compound 6 (100 MHz, CDCl 3

11 Vol. XY, No. 00 Salacia crassifolia (Celastraceae: chemical constituents and antimicrobial activities S11 Figure 20S. DEPT-135 NMR spectrum of compound 6 (100 MHz, CDCl 3 Figure 21S. 1 H NMR spectrum of compound 7 (400 MHz, CDCl 3

12 S12 Rodrigues et al. Quim. Nova Figure 22S. 13 C NMR spectrum of compound 7 (100 MHz, CDCl 3 Figure 23S. DEPT-135 NMR spectrum of compound 7 (100 MHz, CDCl 3

13 Vol. XY, No. 00 Salacia crassifolia (Celastraceae: chemical constituents and antimicrobial activities S13 Figure 24S. 1 H NMR spectrum of compound 8 (400 MHz, CDCl 3 Figure 25S. 13 C NMR spectrum of compound 8 (100 MHz, CDCl 3

14 S14 Rodrigues et al. Quim. Nova Figure 26S. DEPT-135 NMR spectrum of compound 8 (100 MHz, CDCl 3 Figure 27S. 1 H NMR spectrum of compound 9 (400 MHz, CDCl 3

15 Vol. XY, No. 00 Salacia crassifolia (Celastraceae: chemical constituents and antimicrobial activities S15 Figure 28S. 13 C NMR spectrum of compound 9 (100 MHz, CDCl 3 Figure 29S. DEPT-135 NMR spectrum of compound 9 (100 MHz, CDCl 3

16 S16 Rodrigues et al. Quim. Nova Figure 30S. 1 H NMR spectrum of compound 10 (400 MHz, CDCl 3 Figure 31S. 13 C NMR spectrum of compound 10 (100 MHz, CDCl 3

17 Vol. XY, No. 00 Salacia crassifolia (Celastraceae: chemical constituents and antimicrobial activities S17 Figure 32S. DEPT-135 NMR spectrum of compound 10 (100 MHz, CDCl 3 Figure 33S. 1 H NMR spectrum of compound 11 (400 MHz, CDCl 3

18 S18 Rodrigues et al. Quim. Nova Figure 34S. 13 C NMR spectrum of compound 11 (100 MHz, CDCl 3 Figure 35S. DEPT-135 NMR spectrum of compound 11 (100 MHz, CDCl 3

19 Vol. XY, No. 00 Salacia crassifolia (Celastraceae: chemical constituents and antimicrobial activities S19 Figure H NMR spectrum of compound 12 (400 MHz, CDCl 3 Figure 37S. 13 C NMR spectrum of compound 12 (100 MHz, CDCl 3

20 S20 Rodrigues et al. Quim. Nova Figure 38S. DEPT-135 NMR spectrum of compound 12 (100 MHz, CDCl 3 Figure 39S. 1 H NMR spectrum of compound 13 (400 MHz, CDCl 3 + Pyridine-d5

21 Vol. XY, No. 00 Salacia crassifolia (Celastraceae: chemical constituents and antimicrobial activities S21 Figure 40S. 13 C NMR spectrum of compound 13 (100 MHz, CDCl 3 + Pyridine-d5 Figure 41S. DEPT-135 NMR spectrum of compound 13 (400 MHz, CDCl 3 + Pyridine-d5

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